Detailed Description: XQM-4L Experimental Vertical Planetary Ball
Mill
The XQM-4L is a sophisticated piece of laboratory equipment
designed for high-energy ball milling. It belongs to the category
of planetary ball mills, which are renowned for their ability to
produce extremely fine powders and achieve homogeneous mixing and
mechanical alloying of materials that are difficult to process by
other means.
| Model No. | XQM-0.4 |
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| Volume of each matched Jar | 100ml |
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| Voltage | 220V - 50Hz |
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| Machine Size | 500*300*340mm |
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| Machine Weight | 56 Kg without mill jar |
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| Work mode | 4 jars working together |
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| Mill mode | Dry / wet milling |
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| Speed Frequency | Adjusting |
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| Drive Mode | Gear drive |
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| Rotational Speed | 90-870 r/min, adjusting |
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| revolution: rotation | 1:2.14 |
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| Material Capacity | Material + mill balls < 2/3 volume |
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| Input Granularity Size | < 10mm for soft material, < 3mm for hard material |
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| Output Granularity Size | Minimum 0.1μm |
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| Field of application | Geology, Mining, Metallurgy, Electronics, Construction Material,
Ceramics, Chemical Engineering, Light Industry Medicine, Environmental Protection etc. |
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| Feed material | Soft, hard, brittle, fibrous, cellulose, herb, glass, soil,ore,
pharmacy, chemical, fluorescent, pigment etc. |
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| Type of grinding jars | Stainless steel, zirconia, alumina, nylon, PU, tungsten,PTFE etc.,
vacuum jars are available as well. |
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| Type of grinding medium | Stainless steel balls, zirconia balls, alumina balls, PU balls,
steel carbon balls, tungsten balls, etc. |
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| Max. continuous operating time (full-load) | 72 hours |
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| Interval operation | With direction reversal |
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| Certificate | ISO 9001. CE certificate |
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1. Core Design and Configuration
Vertical Orientation: Unlike traditional horizontal ball mills, the
XQM-4L features a vertical main shaft. This design is compact,
saves bench space, and is well-suited for laboratory environments.
4L Capacity: The "4L" designation refers to the total volume of its
four grinding jars. Typically, it is equipped with four 1-liter
jars, giving a combined maximum volume capacity of 4 liters. It's
crucial to note that for effective milling, jars should only be
filled to about one-third to half of their volume with a mixture of
grinding balls and material.
Planetary Motion Mechanism: This is the heart of the machine. The
mill features a large, rotating sun disk (the main turntable).
Mounted on this sun disk are four planetary disks, each holding one
grinding jar.
- The sun disk rotates in one direction (e.g., clockwise).
- Simultaneously, each planetary disk rotates in the opposite
direction (e.g., counter-clockwise) around its own axis.
- This synchronized, counter-rotational movement is what generates
the high centrifugal forces essential for planetary ball milling.
2. Key Components and Features
a) Grinding Jars: Zirconia Agate
The specification of zirconia agate jars is significant:
- Material: Zirconia agate is a sintered composite material,
primarily composed of zirconium dioxide (ZrO₂), known for its
exceptional properties.
- High Hardness & Wear Resistance: It is extremely hard, making it
ideal for grinding even very hard materials (like ceramics, metals,
and minerals) with minimal jar wear. This prevents contamination of
the sample from abraded jar material.
- Chemical Inertness: Zirconia agate is highly chemically stable and
corrosion-resistant. It is suitable for milling a wide range of
materials, including acidic or alkaline substances, without
reacting with them.
- Smooth Inner Surface: This facilitates easy cleaning and minimizes
material adhesion to the jar walls.
b) Grinding Balls
While the mill is equipped with zirconia agate jars, the grinding
balls can be chosen based on the application. Common materials
include:
- Zirconia: For high-density impact and wear resistance.
- Agate: For high-purity applications where iron contamination must
be avoided (e.g., in geology or ceramics).
- Stainless Steel: For tough materials, though it carries a risk of
iron contamination.
- Tungsten Carbide: For the hardest materials.
c) Control System
The XQM-4L is equipped with a digital control system, typically
featuring an LCD screen.
It allows for precise programming of:
- Milling Speed: Adjustable in RPM (Revolutions Per Minute). This
directly controls the centrifugal force and thus the impact energy
of the balls.
- Milling Time: Can be set from seconds up to hundreds of hours,
often with an auto-reverse function to prevent material caking.
- Pause/Interval Cycles: Some models allow for intermittent milling
(e.g., run for 10 minutes, pause for 2 minutes) to prevent
overheating of sensitive materials.
d) Safety and Operational Features
- Safety Lock & Lid Interlock: The milling chamber is covered by a
robust lid with a safety lock. The machine is designed not to
operate unless the lid is securely closed, protecting the user from
moving parts and potential jar breakage.
- Vibration Damping: The unit is mounted on a sturdy base, often with
rubber feet, to dampen vibrations during high-speed operation,
ensuring stability and reducing noise.
- Emergency Stop Button: For immediate shutdown in case of any
abnormality.
3. Principle of Operation (The "Planetary" Action)
The effectiveness of the XQM-4L stems from the complex motion
inside the jars:
- Centrifugal Forces: As the sun disk and planetary disks rotate in
opposite directions, powerful centrifugal forces are generated.
- Coriolis Effect: This force causes the grinding balls inside the
jars to follow a curved trajectory. They are pinned to the jar wall
for a portion of the rotation, then released and flung across the
jar at high velocity.
- Impact and Friction: The size reduction and mixing occur through a
combination of:
- High-Energy Impact: When the balls collide with the material on the
opposite side of the jar.
- Shear and Friction: As the balls roll and slide against each other
and the jar walls.
This combination of forces results in a much higher milling energy
compared to conventional tumbler or horizontal ball mills, allowing
for faster processing times and finer particle sizes (often down to
the sub-micron or even nano range).

4. Typical Applications
The XQM-4L is used across numerous scientific and industrial fields
for:
- Nano-Material Synthesis: Producing nanoparticles of metals, oxides,
and composites.
- Mechanical Alloying: Creating novel alloy phases from elemental
powder blends that are impossible to form by melting.
- Homogenization: Thoroughly mixing different powders (e.g., ceramics
and polymers) to create composite materials.
- Cell Disruption: Breaking down biological cells to extract
proteins, DNA, and other intracellular components.
- Geology and Ceramics: Preparing finely powdered samples for X-ray
Diffraction (XRD) and other analytical techniques.
- Pharmaceuticals: Reducing particle size of active ingredients to
enhance bioavailability.